Preliminaries

CHAPTER 1
Introduction, Chromatography Theory, and Instrument Calibration

CHAPTER 2
Basic Gas Chromatography

CHAPTER 3
Basic High Performance Liquid Chromatography

CHAPTER 4
Basic Capillary Electrophoresis

-4.1 Introduction and History

-4.2 Electrophoresis and Capillary Electrophoresis

-4.2.1 Electro-Osmotic Flow

-4.2.2.1 Longitudinal Diffusion

-4.2.2.2 Injection Length

-4.2.2.3 Sample Adsorption

-4.2.2.4 Electrodispersion

-4.2.2.5 Joule Heating

-4.2.2.6 Detector Cell Size

-4.3 Samples

-4.3.1 Sample Introduction

-4.3.1.1 Types of Sample Injection

-4.3.1.1.1 Hydro- dynamic Injection

-4.3.1.1.2 Electro- kinetic Injection

-4.3.1.1.3 Field Amplified Sample Stacking

-4.3.2 Sample Purification

-4.4 Methods of Operation

-4.4.1 Capillary Zone Electrophoresis (CZE)

-4.4.2 Miceller Electro- kinetic Chromatography (MEKC)

-4.4.3 Capillary Electro- Chromatography (CEC)

-4.4.4 Capillary Gel Electrophoresis (CGE)

-4.4.5 Capillary Isoelectric Focusing (CIEF)

-4.4.6 Capillary Isotachophoresis (CITP)

-4.5 Detectors

-4.5.1 UV-Vis Spectro- photometry

-4.5.2 Indirect Photometry

-4.5.3 Laser-Induced Fluorescence (LIF)

-4.5.4 Contactless Conductivity

-4.5.5 Mass Spectro- metry

-4.5.5.1 Electro-Spray Ionization (ESI)

-4.5.5.1.1 Fydraulic Interfacing

-4.5.5.1.1.1 Sheath Flow Interface

-4.5.5.1.1.2 Sheathless Flow Interface

-4.5.5.2 Atmospheric Pressure Chemical Ionization (APCI)

-4.6 References

CHAPTER 5
Basic Mass Spectrometry

CHAPTER 6
Fragmentation and Interpretation of Spectra

CHAPTER 7
Proper Laboratory Protocol and Laboratory Experiments

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