CHAPTER 1
Introduction, Chromatography Theory, and Instrument Calibration
CHAPTER 2
Basic Gas Chromatography
CHAPTER 3
Basic High Performance Liquid Chromatography
CHAPTER 4
Basic Capillary Electrophoresis
CHAPTER 5
Basic Mass Spectrometry
5.2 Sample Introduction from GC and Analyte Ionization
--5.2.1.1 Ionization Techniques for Solid Non-Volatile Analytes
-- 5.2.1.2b Chemical Ionization (CI)
-5.2.1.3 Repulsion and Accelerator Plates, Slits, and Electronic Focusing Lens
5.3 The Introduction of Samples from HPLC
-5.3.1 Electro-Spray Ionization (ESI) Sample Introduction
-5.3.2 Matrix Assisted Laser Desorption/ Ionization, MALDI
-5.3.3 Proton Transfer Reaction Ionization (PTR)
-5.3.4 Fast Ion Bombardment (FAB)
5.4 The Introduction of Samples from a Capillary Electrophoresis System
5.5 Common Mass Filters (Mass Analyzers)
-5.5.1 Magnetic sector mass filter
-5.5.3 Quadrupole ion trap mass filter
-5.5.4 Time-of-Flight (TOF) mass filter
-5.5.5 Double Focusing Systems
-5.5.6 Fourier Transform Ion Cyclotron – Mass Spectrometry
-5.5.8 Tandem Mass Spectroscopy
5.7 Three-Dimensional Aspects of GC-MS
CHAPTER 6
Fragmentation and Interpretation of Spectra
CHAPTER 7
Proper Laboratory Protocol and Laboratory Experiments