Preliminaries

CHAPTER 1
Introduction, Chromatography Theory, and Instrument Calibration

CHAPTER 2
Basic Gas Chromatography

CHAPTER 3
Basic High Performance Liquid Chromatography

CHAPTER 4
Basic Capillary Electrophoresis

CHAPTER 5
Basic Mass Spectrometry

CHAPTER 6
Fragmentation and Interpretation of Spectra

6.1 Introduction

6.2 Creation of the Spectra

6.3 Identifying the Molecular Ion Peak

6.4 Use of the Molecular Ion

6.5  Identification of Analytes using Isotopic Ratios

6.6  Fragmentation

6.7  Rearrangements

6.8  Identification of Compounds

6.9  Fragmentation of Hydrocarbons

 6.9.1 Fragmentation of Straight Chain Alkanes

 6.9.2 Fragmentation of Branched Alkanes

 6.9.3 Fragmentation of Cyclic Alkanes

 6.9.4 Fragmentation of Alkenes

 6.9.5 Fragmentation of Aromatics

6.10  Fragmentation of Alcohols

6.11 Fragmentation of Ketones and Aldehydes

 6.11.1 Ketones

 6.11.2 Fragmentation of Cyclic Ketones

 6.11.3 Fragmentation of Aromatic Ketones

 6.11.4 Fragmentation of Aldehydes

6.12 Fragmentation of Carboxylic Acids

6.13 Fragmentation of Ethers

6.14 Fragmentation of Esters

6.15 Fragmentation of Amines

6.16 Fractionation of Amides

6.17 Fragmentation of Nitriles

6.18 Reviewing General Principals

6.19  Searchable Databases

6.20 References

6.21 Problems

6.22 Problem Solutions

CHAPTER 7
Proper Laboratory Protocol and Laboratory Experiments

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